MIL-PRF-9000J(SH)
3.10 2,6-Di-tert-butylphenol (DTBP). The addition of DTBP (Chemical Abstract Service Number 128-39-2) in
any lubricating oil produced under this specification is prohibited. This applies to both surface ship and submarine
use. DTBP shall not be intentionally added to the oil. The level of DTBP, if detected, shall not exceed 10 parts per
million. (see 4.6.7)
3.11 Ozone depleting substances (ODS). The use of ODS in the composition of the lubricating oil under this
specification directly or referenced in any federal test method is hereto prohibited. Environmentally safe and non-
ODS alternative solvents shall be substituted in test methods for any previously specified ODS.
4. VERIFICATION
4.1 Classification of inspections. The inspection requirements specified herein are classified as follows:
a.
Qualification inspection (see 4.2).
b.
Conformance inspection (see 4.5).
4.2 Qualification inspection. Qualification tests shall be conducted at a laboratory satisfactory to the Naval Sea
Systems Command. This inspection shall include the applicable tests delineated in table I or table II, and 4.6.2 to
4.3 Sampling for conformance.
4.3.1 Lot. For purposes of sampling, a lot shall consist of all lubricating oil manufactured as one batch and
offered for delivery at one time.
4.3.2 Sampling for examination of filled containers. A random sample of filled containers shall be selected
from each lot in accordance with ANSI/ASQC Z1.4 at inspection level II to verify compliance regarding fill,
closure, marking, and other requirements not involving tests.
4.3.3 Sampling for tests.
4.3.3.1 Blending tank. A composite sample sufficient for testing with at least 1 gallon to be retained for
possible future testing shall be taken from each lot in accordance with the applicable procedure of ASTM D4057.
4.4 Examination of filled containers. Each sample filled container selected in accordance with 4.3.2 shall be
examined for defects of the container and the closure, for evidence of leakage, and for unsatisfactory markings.
Each container shall also be weighed to determine quantity. Any container in the sample having one or more defects
or under required fill shall be cause for rejection of the container.
4.5 Conformance tests. Each sample selected as specified in 4.3.3.1 shall be tested for those parameters listed
in table III and according to methods in table I and II. To insure that the material is essentially the same as that
given qualification under this specification, it is required that, in addition to conforming to this specification, the
results of conformance tests listed in table III shall not vary from the analysis of the sample submitted for
qualification to an extent greater than the tolerances, if any, shown.
4.5.1 Rejection of lots. If a sample of lubricating oil fails any of the tests, the entire lot represented by that sample
shall be rejected.
4.6 Test procedures.
4.6.1 Tests. Tests shall be run as specified in tables I and II and the following procedures. For purposes of
determining conformance with each requirement, an observed value or calculated value shall be rounded off to the
nearest unit in the last right-hand place of figures used in expressing the limiting value, in accordance with the
rounding-off procedure given in ASTM E29.
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