MIL-PRF-23699G
containing a polymer capable of being broken down by turbulence at high rates of shear;
typical viscosities are 10.7 mm2/s (cSt) at 100 °C and 57 mm2/s (cSt) at 40 °C. ASTM Reference
Fluid A may be obtained from vendors listed in the ASTM D2603 method.
4.4.11 Trace metal content. The trace metal content of the oil for qualification testing shall
be determined both with a Rotating Disc Electrode - Atomic Emission Spectrometer (RDE-AES)
and Inductively Coupled Plasma - Atomic Emission Spectrometer (ICP-AES) spectrometer.
4.4.11.1 Spectrometer standardization. The spectrometer shall be standardized and
correlated in accordance with the JOAP Program Manual, NAVAIR 17-15-50.2 using
MIL-DTL-85694 standards. Immediately after standardizing the spectrometer, five
determinations of the oil for trace metal content shall be performed. The average of the
five determinations shall be reported. Samples requiring trace metal content determinations
may be sent to: Naval Air Station, Hazmart Building 2385, Sample (AIR 4.4.6) NOAP, 22680
Hammond Road, Patuxent River, MD 20670.
4.4.11.2 ICP adjustments. In accordance with ASTM D5185, modifications that allow for
the adjustments in the dilution of the sample are allowed to accurately measure 2 ppm (mg/kg) of
metals in the ICP-AES spectrometer.
4.4.11.3 Trace metal conformance testing option. Trace metal content for conformance
testing (table III) can be tested using either RDE-AES spectrometer or ICP-AES spectrometer for
the same elements outlined in table I.
4.4.12 Corrosion and oxidation stability. The corrosion and oxidation stability test shall be
performed in accordance with ASTM D4636, Alternate Procedure 2, with the following
modifications:
a. Duplicate tests shall be run at three separate tests temperatures, each conducted for a
72 hour-duration, at the bath or block temperatures of: 175 ±2.5 °C, 204 ±2.5 °C, and
218 ±2.5 °C. The individual results shall be reported.
b. A suitable liquid medium or fluidized sand bath heating apparatus may be used in lieu
of an aluminum block heater.
c. After the sample tube has been in a liquid heating medium (or aluminum block) for 15
minutes, connect the dry air supply, adjust the air flow rate, and begin the test time.
d. An electrolytic grade silver test square shall be substituted for the cadmium plated
steel square; in the 218 °C test, substitute titanium conforming to SAE AMS4900 (or
equivalent), for copper and magnesium; stainless steel or nickel-chrome wire may be
used to tie the metal coupons together at all test conditions.
e. Post test oil viscosity sample is compared with viscosity of new oil samples tested at
40 °C . Post test oil total acid number is compared to the total acid number of the
new oil sample. The total acid number shall be determined in accordance with
SAE ARP5088.
f. The glassware from FED-STD-791, method 5308 can be used.
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